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Entry  Monday, August 08, 2016, 15:22, Laura Lambert, SiC, 40860-3, LP-IG-LIS, Problems, Conditioning SiC#34 conditioning_temperature_graph.xlsxstriptool_conditioning_target_BROKEN.JPG
    Reply  Tuesday, August 30, 2016, 15:25, John Wong, SiC, 40860-3, LP-IG-LIS, Problems, Conditioning SiC#34. Note about the p/s voltage Capture.PNG
Message ID: 318     Entry time: Tuesday, August 30, 2016, 15:25     In reply to: 312
Author: John Wong 
Target Material: SiC 
Target Oven W.O#: 40860-3 
Source: LP-IG-LIS 
Status: Problems 
Subject: Conditioning SiC#34. Note about the p/s voltage 

Laura Lambert wrote:

 Monday, August 08, 2016, 15:19

Previously sintered over weekend [see elog i.d 311]

Target container contains 471 discs of SiC [6 x 5 packs + 441 single discs]

Target packed length = 16cm. 

Mass of 533 discs SiC(green)  = 52.7172g

Container is wrapped with 3 heatshields; no end caps are inserted yet - coated spring inserted both sides to hold discs in place.

Conditioning temp = 1800C.

TGHT max = 450A.  TBHT max = 230A. 

Chamber is currently being pumped down. 


 Monday, August 08, 2016, 16:38

Target was not removed from evap2 after sintering, vented and cleaned windows only.

IGP1 = 5.5e-6 Torr

Stepped up manually to 80A, vacuum stable.

IGP1 = 3.2e-6 Torr

Initiating auto-ramp at 0.2A/min for the TGHT and 0.1A/min for the TBHT.


 Thursday, August 11, 2016, 14:14

Tues the TGHT reached ~280A via auto-ramp

Evap2 was then tapped up manually to 480A/ ~1800C

Temperature readings on OMEGA have fluctuated up and down during conditioning process which was also observed for SiC#33

Also consistent with SiC#33, a lower current was required to reach 1800C during the conditioning process compared to the sintering process.

See attached link for data.


 Tuesday, August 16, 2016, 16:25

TGHT remained at 480A, 9.2V for ~7 days.

IGP1 = 6.5e-6 Torr

OMEGA = 1470C [with window coating, so temperature reading compromised]

Initiating auto cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.


Wednesday, August 17, 2016, 13:40

Vented in air and opened this morning.

Target broke  

Target clearly heated to high.

See attached snapshot of striptool from conditioning process.

Will update later with photos of broken container


 

 Tuesday, August 30, 2016, 15:17

A better look at the p/s voltage over the course of the constant heating at 480A.  (see attachment).

The striptool shows the voltage was not giving a stable output.  There were multiple occasions that the voltage dropped and then recovered; the obvious was on Aug 16.  This indicates that  the target was breaking up.

Finally on Aug 17, the voltage dropped and never recovered again - that indicates the target was broken.

Attachment 1: Capture.PNG  28 kB  | Show | Show all
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