Friday, February 12, 2016, 11:01
Container coated with TaC with new method - ends tapped off, liquid poured/swirled around container, then poured back out - 'flushing technique'.
Container wrapped with 3 x Ta heat shields, incl center block - new method of each layer being one long single Ta foil covering entire container incl center block
IGP1 = 6.3e-7Torr
HS water valves opened, no leaks detected.
Tapped up manually to 35A.
Waited ~20min.
Vacuum stable, IGP1 = 1.3e-6 Torr.
Initiated auto-ramp at 0.2A/min and 0.1A/min for the TGHT and TBHT respectively with final setpoints of 400A and 230A.
Monday, February 15, 2016, 08:56
IGP1 = 3.9e-7 Torr.
TBHT = 230A, 4.0V
TGHT = 400A, 6.58V
OMEGA = 1766C
Tapping up manually to 1900C...
Monday, February 15, 2016, 10:18
IGP1 = 5e-7 Torr
TGHT = 450A, 7.55V
OMEGA = 1913C
Monday, February 15, 2016, 14:30
IGP1 = 4.9e-7 Torr.
TGHT = 450A, 7.55V.
Material remained at ~1910C for ~4hrs.
Initiating auto-cool at 2.0A/min and 1.0A/min for the TGHT and TBHT respectively.
Tuesday, February 16, 2016, 14:17
vented in air and opened up this morning.
target container sintered nicely.
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