John Wong wrote: |
Tuesday, September 01, 2015, 17:16
Target container contains 533 discs of SiC with packed length of 17cm.
Mass of 533 discs SiC(green) = 57.8979g
Total mass SiC(green) + target container = 1455g
Container is wrapped with 3 heatshields; no end caps are inserted yet.
Sintering temp at 1800C - TGHT will be set accordingly. TBHT max at 230A.
Chamber is currently being pumped down.
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Wednesday, September 02, 2015, 09:11
HS water valves opened, no leaks detected.
IGP1 = 1.15e-6 Torr
Tapped up manually to 40A.
Waited ~1hr40 for vacuum to stabilize.
IGP1 = 3.6e-6 Torr.
Max setpoints set to TGHT = 630A and TBHT = 230A, ~1400C
Initiating auto ramp at a rate of 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.
Once max setpoints achieved, will tap up manually until window port becomes coated [as previously observed]
Once window port becomes coated will leave at set temp for ~4hrs to continue with outgassing, then cool down, clean window and ramp back up.
If LS port still clean, will continue to ramp up to final desired temperature of 1800C.
Wednesday, September 02, 2015, 14:23
IGP1 = 4.0e-5 Torr.
Vacuum too high, stopped auto-ramp and tapped down manually.
Dropped TGHT down from 80A to 50A
Dropped TBHT down from 55A to 50A
Wednesday, September 02, 2015, 15:29
Vacuum down to IGP1 = 1.2e-5 Torr.
Re-initiating auto-ramp...
Tuesday, September 08, 2015, 10:04
IGP1 = 4.5e-7 Torr.
TGHT = 630A, 9.6V
TBHT = 230A, 3.2V
DV = 0.22V
OMEGA RS = 1476C
OMEGA LS = 1450C
see attached photo for screenshot.
will tap up manually with a visual on both window ports...
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