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Entry  Tuesday, September 01, 2015, 17:20, John Wong, SiC, 39530-5, HP-FEBIAD, In progress, Sintering SiC#32 
    Reply  Wednesday, September 02, 2015, 11:28, Laura Lambert, SiC, 39530-5, HP-FEBIAD, In progress, Sintering SiC#32 Screenshot-1stsintering-prewindow_coating.JPG
       Reply  Tuesday, September 08, 2015, 15:56, John Wong, SiC, 39530-5, HP-FEBIAD, In progress, Sintering SiC#32 SiC#33_HPFEBIAD_temp.PNGSiC#33_HPFEBIAD_temp.xlsxleft_window.JPGleft_window_1.JPG
          Reply  Wednesday, September 09, 2015, 18:24, John Wong, SiC, 39530-5, HP-FEBIAD, In progress, Re-conditioning SiC#32 Screen_Shot_2015-09-09_at_5.53.15_PM.png
             Reply  Thursday, September 10, 2015, 09:58, Laura Lambert, SiC, 39530-5, HP-FEBIAD, In progress, Re-conditioning SiC#32 
                Reply  Thursday, September 10, 2015, 12:05, John Wong, SiC, 39530-5, HP-FEBIAD, Done, Re-conditioning SiC#32 Screen_Shot_2015-09-15_at_12.37.19_PM.pngScreen_Shot_2015-09-18_at_9.10.13_AM.pngScreen_Shot_2015-09-24_at_11.30.25_AM.png
Message ID: 244     Entry time: Wednesday, September 02, 2015, 11:28     In reply to: 243     Reply to this: 245
Author: Laura Lambert 
Target Material: SiC 
Target Oven W.O#: 39530-5 
Source: HP-FEBIAD 
Status: In progress 
Subject: Sintering SiC#32 

John Wong wrote:

Tuesday, September 01, 2015, 17:16

Target container contains 533 discs of SiC with packed length of 17cm. 

Mass of 533 discs SiC(green)  = 57.8979g

Total mass SiC(green) + target container = 1455g

Container is wrapped with 3 heatshields; no end caps are inserted yet.

Sintering temp at 1800C - TGHT will be set accordingly.  TBHT max at 230A. 

Chamber is currently being pumped down. 


 

 Wednesday, September 02, 2015, 09:11

HS water valves opened, no leaks detected.

IGP1 = 1.15e-6 Torr

Tapped up manually to 40A.

Waited ~1hr40 for vacuum to stabilize.

IGP1 = 3.6e-6 Torr.

Max setpoints set to TGHT = 630A and TBHT = 230A, ~1400C

Initiating auto ramp at a rate of 0.2A/min and 0.1A/min for the TGHT and TBHT respectively.

Once max setpoints achieved, will tap up manually until window port becomes coated [as previously observed]

Once window port becomes coated will leave at set temp for ~4hrs to continue with outgassing, then cool down, clean window and ramp back up.

If LS port still clean, will continue to ramp up to final desired temperature of 1800C.


 Wednesday, September 02, 2015, 14:23

IGP1 = 4.0e-5 Torr.

Vacuum too high, stopped auto-ramp and tapped down manually.

Dropped TGHT down from 80A to 50A

Dropped TBHT down from 55A to 50A


Wednesday, September 02, 2015, 15:29

Vacuum down to IGP1 = 1.2e-5 Torr.

Re-initiating auto-ramp...


 Tuesday, September 08, 2015, 10:04

IGP1 = 4.5e-7 Torr.

TGHT = 630A, 9.6V

TBHT = 230A, 3.2V

DV = 0.22V

OMEGA RS = 1476C

OMEGA LS = 1450C

see attached photo for screenshot.

will tap up manually with a visual on both window ports...


 

Attachment 1: Screenshot-1stsintering-prewindow_coating.JPG  256 kB  Uploaded Tuesday, September 08, 2015, 11:08  | Show | Hide all
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