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Entry  Friday, July 31, 2015, 15:51, John Wong, Ta, , TARGET BOAT, In progress, Test for homogeneity: Sintering TaC coating on a Ta tube Screen_Shot_2015-07-31_at_3.46.10_PM.png
    Reply  Tuesday, August 04, 2015, 12:04, Laura Lambert, Ta, , TARGET BOAT, Done, Test for homogeneity: Sintering TaC coating on a Ta tube Temp_measurements_of_new_port_window_for_2nd_OMEGA.xlsxIMG_20150806_151719182.jpgIMG_20150806_151748536.jpg
Message ID: 234     Entry time: Tuesday, August 04, 2015, 12:04     In reply to: 233
Author: Laura Lambert 
Target Material: Ta 
Target Oven W.O#:  
Source: TARGET BOAT 
Status: Done 
Subject: Test for homogeneity: Sintering TaC coating on a Ta tube 

John Wong wrote:

 Friday, July 31, 2015, 15:39

A Ta tube was coated with TaC.  The inner of the tube was filled with TaC solution and the excess was drained out to give a homogenous coating.  The outer layer of the tube was brushed with TaC. 

The tube is installed in a target boat and wrapped with 3 layers of heat shields.  

Chamber is currently pumped down and the target heater will be ramped up after the long weekend (Tue)

A new window port is installed (see photo).  TGHT will need to be ramped up slowly to make sure the new window can sustain the heat shine from the target - local check on the Evap is required to make sure it's safe to keep ramping up the heater.     


 

Tuesday, August 04, 2015, 11:26

HS water valves opened, no leaks detected.

IGP1 = 2.2e-7 Torr.

Tapped up manually to 30A.

IGP1 = 2.7e-7 Torr.

Initiating auto-ramp at 0.2A/min with a final value of 350A.


 Tuesday, August 04, 2015, 15:30

IGP1 = 2.8e-6 Torr.

TGHT = 79A.

Increasing ramping rate to 0.5A/min


 Wednesday, August 05, 2015, 15:25

EVAP2 reached 350A this morning, OMEGA = 1414C

Temperature measurements were taken using the FLUKE IR camera of the new window port to be used for the second OMEGA camera.

Measurements were taken of both the Cu seal on the inside of the window and in the centre of the window [the hottest point].

TGHT was ramped up at 2.0A/min from 1414C --> 1800C with auto ramp paused at each measurement reading taken.

See attachment for raw data.

TGHT remained at 500A/1800C for 4hrs and will be cooled down at a rate of 2.0A/min.


 Thursday, August 06, 2015, 15:32

Vented and opened today.

New window port passed inspection, max temperature reached = 32.4C

Coating on tube looks good, partial sintering. Internal sintered better than outside of tube.

See attached photos.


 

Attachment 1: Temp_measurements_of_new_port_window_for_2nd_OMEGA.xlsx  12 kB  Uploaded Wednesday, August 05, 2015, 16:29
Attachment 2: IMG_20150806_151719182.jpg  2.588 MB  Uploaded Thursday, August 06, 2015, 16:33  | Hide | Hide all
IMG_20150806_151719182.jpg
Attachment 3: IMG_20150806_151748536.jpg  2.345 MB  Uploaded Thursday, August 06, 2015, 16:34  | Show | Hide all
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