Tuesday, January 28, 2014, 15:43
The target containers end-caps were coated with TaC spray and let dry.
Each cap is wrapped with a small piece of graphite foil and inserted in the target boat. [see attached photo]
The chamber is currently being pumped down overnight.
Wednesday, January 29, 2014, 11:32
Chamber was pumped down to 1.6e-7 Torr overnight.
HS cooling water valve opened; no leaks detected.
TGHT was stepped up to 35A, voltage max set at 11.05V. TBHT currently at 0A.
Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min and max setpoint to 580A.
Good vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.
Thursday, January 30, 2014, 09:06
TGHT has been slowly ramping up overnight at a rate of 0.2A/min.
IGP1 = 2.4e-7 Torr, TGHT = 283A; stepping ramping rate up to 2.0A/min.
Thursday, January 30, 2014, 15:53
TGHT reached 580A at 11:45. Measured temp @1650C.
Initiating TGHT auto-cooling now at 2.0A/min.
Friday, January 31, 2014, 09:04
Chamber cooled down overnight, vented and opened this morning.
Smooth run!
Friday, January 31, 2014, 11:21
Opened up the end caps, turns out it wasn't such a smooth run...they're not fully sintered
See attached photo comparison between fully sintered end cap [silver] and end cap from this run [green].
Will re-install and re-sinter next week.
Wednesday, February 05, 2014, 11:34
End-caps re-installed into EVAP2
Target boat is wrapped with 3 x Ta heat-shield.
Chamber is currently being pumped down.
Wednesday, February 05, 2014, 14:31
Chamber was pumped down to 5e-7 Torr this morning.
HS cooling water valve opened, no leaks detected.
TGHT was stepped up to 35A, voltage max set at 11.05V. TBHT currently at 0A.
Waited ~20min, current stabilized, vacuum started to drop, auto-ramp initiated at 0.2A/min and max setpoint to 580A.
Good Vacuum: 3.00e-5 Torr, Bad vacuum 4.00e-5 Torr.
Thursday, February 06, 2014, 09:06
TGHT has been slowly ramping up overnight at a rate of 0.2A/min.
IGP1 = 1.1e-7 Torr, TGHT = 259A; stepping ramping rate up to 2.0A/min.
Friday, February 07, 2014, 10:10
TGHT reached 580A yesterday. Measured internal temp @ 1500C.
Initiated TGHT auto-cooling this morning at 2.0A/min
Tuesday, February 11, 2014, 13:30
Vented and opened chamber this morning.
Endcaps are toast [see pictures attached]
Some of the endcaps broke/fried, others deformed-none useable.
Possibly due to new target boat resulting in more current?
Too much heat with Ta heat shields?
Bad News Bears
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