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Entry  Friday, July 04, 2014, 10:23, John Wong, ThO2, 40282-2, TARGET BOAT, Done, Test: Sintering ThO2 with Nb backing foils  2014-07-03_12.29.29.jpgThO_raw_green_sintered_30um.pngpressure_current_plot.PNG
    Reply  Wednesday, July 09, 2014, 13:57, Laura Lambert, ThO2, 40282-2, TARGET BOAT, Done, Test: Sintering ThO2 with Nb backing foils  test_batch_full_sintering.JPGjul9_2014_(2).jpg
Message ID: 97     Entry time: Wednesday, July 09, 2014, 13:57     In reply to: 96
Author: Laura Lambert 
Target Material: ThO2 
Target Oven W.O#: 40282-2 
Source: TARGET BOAT 
Status: Done 
Subject: Test: Sintering ThO2 with Nb backing foils  

John Wong wrote:

Friday, July 04, 2014, 10:13

Target boat contains 4 set of samples.  Each sample consists of 5pack ThO2/Nb.  (see photos).

The container is wrapped with 3 layers of heat shield. 

TGHT will be ramped up to 520A at 0.1A/min.

Chamber has been pumped over night, pressure at 4.20e-6 Torr.

The purpose of this test:

1.  Will the Ta- target boat survive at that current?

2.  How will ThO2 sintered?  Shrinkage? Grain-growth? mass loss? density? SEM will be done later.

3.  How will the pressure behave at the max operating temperature (or current)?


  Friday, July 04, 2014, 12:29

Stepped up TGHT to 40A,  Vac went to max at 3.5e-5 Torr and is coming down.

Auto-ramping initiated. 


 

Wednesday, July 09, 2014, 13:55

TGHT reached 520A tuesday morning. [see attached archive screenshot]

Initiated auto-cool at 1.0A/min tuesday afternoon.

Vented in air and took samples out of EVAP1 wednesday morning. [see attached sample photo]


 

Attachment 1: test_batch_full_sintering.JPG  91 kB  Uploaded Wednesday, July 09, 2014, 14:58  | Show | Show all
Attachment 2: jul9_2014_(2).jpg  2.225 MB  Uploaded Wednesday, July 09, 2014, 15:00  | Show | Show all
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