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Message ID: 81     Entry time: Friday, October 11, 2013, 18:10
Author: John Wong 
Target Material: UC2 
Target Oven W.O#: 39814-IV 
Source: LP-IG-LIS 
Status: Done 
Subject: UCx#8 - Final Conditioning 

 Friday, October 11, 2013, 18:00

 

The target container was previously coated with TaC and sintered in Evap 2.

The target is loaded with ??? discs of UCx (material from batch #???)

Total length = ???

The container is wrapped with 3 layers of Ta-heat shield, including the back block.

A regular TaC coated / sintered endcap is inserted on left, wrt the ionizer tube pointing out of the page. The right end is open with no cap.

The chamber is pumping down.


Instructions for conditioning the UCx target:

1. TGHT will need to heat up to ~ 175A to burn off the organics.

    Parameter setup: 5.0e-5 good vac, 6.0e-5 bad vac. The auto-ramping rate is set to 0.1A/min.

2. Once the organics have burnt off, ramp down the TGHT to 0A at 2A/min.

3. Purge the glovebox with argon gas.

4. Vent the chamber with Ar gas. Close the valve when it is completely vented.

5. Remove the target. Be careful the left end (view from the top) is open with the D-cap.

6. Clean the chamber with TCE and remove all the gunge.

7. Install the target back

8. Pump down the chamber to at least low 10e-6 Torr before begin the final carbonization process.

9. Auto-ramp the TGHT current to 175A at 1A/min.

10. Once the TGHT reach to 175A. Auto-ramp TGHT to 520A at 0.1A/min.

11. At 520A, keep heating the target for at least 4-5 hours.

12. Auto ramp TGHT to 0A at 2A/min.

13. Purge the glovebox with argon for at least 5 min.

14. Vent the chamber with argon gas. Close the valve when it is completely vented.

15. Remove the target from the chamber and put in the "orange james bond box" and transport to the Ar-glove box.


Friday, October 11, 2013, 18:03 
 
Chamber has been pumping down, IG1 currently at 1.58e-6 Torr.
 
TGHT stepped up to 25A and auto ramping initiated... 

 Monday, October 21, 2013, 11:29
 
TGHT to max current at 520A and heated for about 2 days (over the weekend).
 
IG came down to 4.6 e-6 Torr.
 
Cooling down initiated at 2A/min.

 

 

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