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Message ID: 38     Entry time: Tuesday, September 13, 2011, 16:53
Author: John Wong 
Target Material: SiC 
Target Oven W.O#: 38295-9 
Source: HP-FEBIAD 
Status: Done 
Subject: Ready  

Tuesday, September 13, 2011, 16:51

Target is wrapped with 3-Ta heat shields. 

Loaded with 555 SiC discs (total mass 64.24g)

18cm in length.

D-end cap on one end, and a regular end end on the other.

Chamber is currently being pump down


 Wednesday, September 14, 2011, 09:58

Evaporator has been pumped down over night, currently IG @ 1.71e-6 Torr. BP @ 23mT.

The target will be heated up to 550A and will wait to see any reaction happen before increasing TGHT (Max 820A).

TGHT stepped up to 90A, local @ 87A.  Pressure slowly rising, IG @ 2.7e-6 Torr. BP @ 23mT. 

Start auto-heating @ 0.5A/min to max TGHT @ 500A.  


 Friday, September 16, 2011, 00:27:

TGHT @ 250A and pressure has already started to come down, currently at 2.8e-5 Torr.  

Increased TGHT rate from 0.5A/min to 2A/min, and pressure started to rise.  Stopped auto-ramping after pressure increased to 4.4e-5 Torr.  (see attachment#1: TGHT_270A-300A.jpg).

Decreased TGHT rate back to 0.5A/min and changed pressure limit to 3.0e-5 Torr.  


Friday, September 16, 2011, 01:49 :

TGHT @ 347A, and pressure seems to come down slowly. 

Change TGHT auto heating to 550A and pressure limit at 2.5e-5 Torr.  Vac currently at 2.4e-5 Torr.  Ramping rate at 0.5A/min. 


Friday, September 16, 2011, 10:58  

TGHT reached 580A and no spike in the vacuum.  Ramping up TGHT to 590A, keeping pressure limit @ 1.35e-5 Torr,

Currently IG @ 1.33 e-5 Torr.  Current TGHT @ 585.5A, local @  579A.

(see attachment 3: TGHT_580A)


Friday, September 16, 2011, 11:35:

TGHT reached to 590A, not much of out-gassing.  Pressure increased from 1.30e-5 Torr to 1.40e-5 Torr.  

Continue ramping up TGHT, set to 700A, pressure limiting @ 1.5e-5 Torr.


Friday, September 16, 2011, 15:29:

TGHT reached to 700A, local @ 692A; pressure was stable at 1.38e-5 Torr throughout the whole time.  

Continues ramping up TGHT to 820A (max) at 0.5A/min; pressure limiting @ 1.5e-5 Torr. 


Friday, September 16, 2011, 22:05 

TGHT reached to 820A (local 810A) and held for ~3hrs.  IG @ 5.4e-6Torr and coming down, BP @ 20mT. 

See attachment#4:  TGHT_820A.

TGHT cooling down begins... 


 Monday, September 19, 2011, 10:08

TGHT was cooled down over the weekend. 

See attachment#4: archiver_TGHT_0-820A. 

Currently, IG @ 6.9e-7 Torr, BP @ 27mT.

Evaporator will be vented. 


Tuesday, September 20, 2011, 08:51 

Target turned out well.  

D-cap was removed and replaced with a regular TaC-coated sintered endcap with a graphite foil.  

See attachments for details.

Target is now ready for assembly and test for test-stand. 

 


 

Attachment 1: TGHT_270A-300A.jpg  24 kB  Uploaded Friday, September 16, 2011, 01:33  | Show | Hide all
Attachment 2: TGHT_347A.jpg  24 kB  Uploaded Friday, September 16, 2011, 02:52  | Show | Hide all
Attachment 3: TGHT_580A.JPG  58 kB  Uploaded Friday, September 16, 2011, 12:02  | Show | Hide all
Attachment 4: TGHT_820A.jpg  22 kB  Uploaded Friday, September 16, 2011, 23:14  | Show | Hide all
Attachment 5: archiver_TGHT_0-820A.JPG  67 kB  Uploaded Monday, September 19, 2011, 11:10  | Show | Hide all
Attachment 6: D-cap_outgassing.jpg  1.900 MB  Uploaded Tuesday, September 20, 2011, 09:53  | Show | Hide all
Attachment 7: D-endcap_aftersintering.jpg  1.782 MB  Uploaded Tuesday, September 20, 2011, 09:53  | Show | Hide all
Attachment 8: Sintered_SiC_&_newcap.jpg  1.218 MB  Uploaded Tuesday, September 20, 2011, 09:54  | Show | Hide all
Attachment 9: SiC_TGHT0-820A.jpg  207 kB  Uploaded Tuesday, September 20, 2011, 09:55  | Hide | Hide all
SiC_TGHT0-820A.jpg
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