Wednesday, October 11, 2023, 9:36
Cartridge #10 loaded with 213 plus 3 analysi discs
To be reduced inside a Ta container tube. Tube wrapped in 3 Ta foil heatshields.
Reduction for 4 hours and then 8 hours @ 450A
Good Vacuum: 5.0e-04 Torr
Bad Vacuum: 5.0e-02 Torr
Initial pressure is 2.4 e-06 Torr
Wednesday, October 11, 2023, 10:56
Starting heat ramp at 2A/min to 60A
First pressure bump observed at 60A
Allowing pressure to restabilize
Wednesday, October 11, 2023, 13:12
IGP1=2.6 e-5 Torr
continuing to heat at 2A/min
Wednesday, October 11, 2023, 13:35
another pressure bump observed around 90A (should go slowly in these current range). Aborted ramp, waiting for pressure to stabilize.
pressure rose to around 2.5e-02 Torr (close to our bad pressure)
Wednesday, October 11, 2023, 13:52
IGP1=5.4e-04 Torr Start ramp at 2A/min
Wednesday, October 11, 2023, 17:53
Pressure has started to drop so increased ramp to 4A/min
Wednesday, October 11, 2023, 18:18
Second small pressure bump observed at 482A and 5.0 V. Pressure falling. Will leave at 500A for 4 hours .
Wednesday, October 11, 2023, 22:00
IGP1= 8.0 e-06 Torr
TGHT=500A, 5.2V
Initiate rampdown to 450A and will leave there for 8 hours
Thursday, October 12, 2023, 07:02
Initiate rampdown to zero. IGP1=3.21e-06 Torr
TGHT= 450A, 4.6V |