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Entry  Thursday, January 30, 2020, 09:37, Marla Cervantes, UO2/C, P2N-02, , In progress, P2N target material carbothermal reduction 
    Reply  Thursday, January 30, 2020, 10:15, Marla Cervantes, UO2/C, P2N-02, , Problems, P2N target material carbothermal reduction 
       Reply  Thursday, January 30, 2020, 11:53, Marla Cervantes, UO2/C, P2N-02, , Problems resolved, P2N target material carbothermal reduction 
          Reply  Thursday, January 30, 2020, 13:11, Marla Cervantes, UO2/C, P2N-02, , Problems, P2N target material carbothermal reduction voltage-rising.JPG
             Reply  Friday, January 31, 2020, 15:36, Marla Cervantes, UO2/C, P2N-02, , Done, P2N target material carbothermal reduction P2N-Carbothermal_reduction.JPG
                Reply  Thursday, August 13, 2020, 14:37, Marla Cervantes, UO2/C, P2N-02, , Problems, P2N target material carbothermal reduction 200815-Vacuum_P2N.PNG
                   Reply  Tuesday, August 18, 2020, 20:45, Marla Cervantes, UO2/C, P2N-02, , Problems resolved, P2N target material carbothermal reduction 
Message ID: 254     Entry time: Thursday, January 30, 2020, 09:37     Reply to this: 255
Author: Marla Cervantes 
Target Material: UO2/C 
Target Oven W.O#: P2N-02 
Source:  
Status: In progress 
Subject: P2N target material carbothermal reduction 

Wednesday, January 29 2020, 05:55  

A P2N container  with heat shields, and with a UO2/C loaded graphite container was installed in the EVAP1

Chamber is currently being evacuated.


Thursday, January 30, 2020, 08:56

Pressure limits:

Good vacuum 1e-1 Torr

Bad vacuum 5e-1 Torr

Initial pressure: 

IGP1=1.52e-6Torr

Current ramp set to 1A/min to 10 A, voltage is stable.

Current ramp increased to 1A/10s to 100 A. The pressure started raising around 80 A.

Current was kept 5min at at 100 A, voltage was stable


Thursday, January 30, 2020, 09:32 

Current ramp set to 1A/20s to 150 A (same pressure limits)

Pressure keep increasing during heating


Thursday, January 30, 2020, 09:53 

Current was kept at 150 min during 5 min, the voltage is stable, pressure started to stabilize:

IGP1 = 0.027 Torr

TGHT = 0.418 V

Ramp set to 1A/min to 200 A.


Thursday, January 30, 2020, 10:02

Pressure decreasing:

TGHT= 153 A 

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