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Entry  Monday, October 28, 2019, 11:23, Marla Cervantes, UO2/C, , TARGET BOAT, In progress, UCx#30 Carbothermal Reduction UCx30-CarbothramlReduction.JPGUCx30-CurrentDrop.JPG
    Reply  Thursday, October 31, 2019, 13:59, Marla Cervantes, UO2/C, , TARGET BOAT, Problems, UCx#30 Carbothermal Reduction 
Message ID: 248     Entry time: Monday, October 28, 2019, 11:23     Reply to this: 249
Author: Marla Cervantes 
Target Material: UO2/C 
Target Oven W.O#:  
Source: TARGET BOAT 
Status: In progress 
Subject: UCx#30 Carbothermal Reduction 

Monday, October 28, 2019, 10:29

A loaded graphite cartridge was set in a tantalum boated and wrapped with 3 tantalum sheets

The set up was installed in the EVAP1 and pumped dwon during the weekend.

IGP1 = 1.10 e-6 Torr


Monday, October 28, 2019, 10:31

Good vacuum = 1e-1 Torr

Bad vaccum = 5e-1 Torr

The current ramp is 1 A each 10 s from 0 A to 100 A


Monday, October 28, 2019, 11:13 

After 18 min the pressure started dropped.


Monday, October 28, 2019, 11:22 

When the pressure reduced to 5e-4 Torr the current ramp was changed to 3.3 A each 10 s to 480 A, the vacuum limits stayed the same.


Monday, October 28, 2019, 11:45

The limit was set to 500 A with same ramp


Monday, October 28, 2019, 11:48 

The ramp was changed to 1A/10s to 550 A


 Monday, October 28, 2019, 11:55

At 520 A the pressure reach 1e-1 Torr and the autoramp stopped


Monday, October 28, 2019, 13:39

the current was increased manually at aprox. 1A/30 s 

The current dropped suddenly even though the pressure was under the limits and the ramping was in the limits.

Autoramp was set to 3 A/ 10 s from to to 500 A

Then it was changed to 1 A  /30s from 500 to 506 A

Finally it was changed to 1 A/ 10 s from 506 to 520 A

Manually tapped to 530 A


Monday, October 28, 2019, 15:40

At 13:45 the current reached 530 A. 

Attachment 1: UCx30-CarbothramlReduction.JPG  62 kB  Uploaded Monday, October 28, 2019, 12:58  | Hide | Hide all
UCx30-CarbothramlReduction.JPG
Attachment 2: UCx30-CurrentDrop.JPG  59 kB  Uploaded Monday, October 28, 2019, 13:09  | Show | Hide all
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