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Message ID: 236     Entry time: Friday, April 05, 2019, 10:08
Author: Marla Cervantes 
Target Material:  
Target Oven W.O#: 43630-3 
Source:  
Status: Done 
Subject: TaC coating/sintering for graphite insert test 

 Friday, April 05, 2019, 10:04

A tantalum tube was coated with TaC and wrapped with Ta heat-shield (3 layers)

Desired temp = 1900 C (expected TGHT ~445A/7.5V), TBHT will be set fixed at 230A (max).

Yesterday the tube was set in the EVAP1 and pumped down.


Friday, April 05, 2019, 10:07 

IGP1= 1.61e-6 Torr

The current is manually tapped to 40 A.


Friday, April 05, 2019, 13:25

After ~2 hours 

IGP1 = 1.54e-6 Torr

TGHT = 0.61 V, 40.39 A

Autoramp is set to 1 A/min to 400 A

Good vac at 3.00-5 Torr

Bad vac at 5.0e-5 Torr.


Sunday, April 07, 2019, 9:00

The current was increased to 424 A


Monday, April 08, 2019, 16:36

EVAP1 vented with air, sintered tube was removed. 

Attachment 1: EVAP1-TaC_Coating.JPG  47 kB  Uploaded Thursday, May 09, 2019, 11:23  | Hide | Hide all
EVAP1-TaC_Coating.JPG
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