Thursday, July 05, 2018, 13:24
Target container was previously coated and sintered with TaC, also wrapped with Ta heat shields (see Evap2 elog# 410).
Loaded 201 discs of UCx with 7.27 cm in length + 5 extra discs for QC samples.
One end-cap (coated/sintered TaC) inserted right, wrt the ionizer tube pointing down.
Left side is OPEN; a spring is inserted to hold the discs in place.
Chamber is currently being pumped down.
TGHT will be ramped up to 495A/8.85V and TBHT to 230A/3.26V (same parameters used for sintering the container, evap2 elog#410).
Vacuum initial setting:
Good Vac = 5.0 e-5 Torr, Bad vac = 8.0 e-5 Torr.
pressure level will be monitored accordingly...
Auto-ramping setting
TGHT: 60 wait time, 0.2A/min, final 495A
TGHT: 60 wait time, 0.2A/min, final 230A.
Thursday, July 05, 2018, 16:50
Tapping up TGHT to 40 A/0.49 V and TGHT to 40A/0.64V.
Vac slowly increasing from 5.0 e-6 Torr.
Initiate auto-heating
Tuesday, July 10, 2018, 10:46
Holding TGHT at 495A/5.3V for over 25 hours. Pressure at 2.9e-6 Torr.
Initiate autocooling TGHT at 2A/min, TBHT 1.0A/min
Wednesday, July 11, 2018, 17:12
Target was removed from the Evap; it is now in the Ar glovebox. End cap is inserted.
Target is ready for installation.
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