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Entry  Wednesday, March 28, 2018, 11:46, Laura Lambert, UO2/C, 40282-2, TARGET BOAT, In progress, Carbonizing first full length 1step UCx target 
    Reply  Monday, April 09, 2018, 16:51, Laura Lambert, UO2/C, 40282-2, TARGET BOAT, Problems, Carbonizing first full length 1step UCx target evap1_trip.JPGevap1_trip_archive.JPG
       Reply  Monday, April 09, 2018, 16:53, Laura Lambert, UO2/C, 40282-2, TARGET BOAT, Problems resolved, Carbonizing first full length 1step UCx target 
          Reply  Tuesday, April 10, 2018, 14:49, Laura Lambert, UO2/C, 40282-2, TARGET BOAT, Done, Carbonizing first full length 1step UCx target 
Message ID: 199     Entry time: Wednesday, March 28, 2018, 11:46     Reply to this: 200
Author: Laura Lambert 
Target Material: UO2/C 
Target Oven W.O#: 40282-2 
Source: TARGET BOAT 
Status: In progress 
Subject: Carbonizing first full length 1step UCx target 

 Wednesday, March 28, 2018, 11:35

D-shaped discs were cut from cast 2, the same as the last sample of 1stepUCx [see elog i.d. 197]

A 13mm punch was used to punch out discs from pre-cut strips using the old method.

The target consists of 195 discs with 8.1cm in length - all single discs, no packs.

195 x UO2/C discs = 19.79g

Graphite insert is placed inside a target boat with both endcaps on.

Boat previously coated with TaC and sintered.

Ta-target boat is wrapped with 3-layers of heat shield and installed in evap1 yesterday afternoon.

Chamber pumped down overnight.


 Wednesday, March 28, 2018, 13:33

IGP1 = 4.03e-7 Torr

Tapped up TGHT manually to 80A, 0.83V - waited 50min, vacuum started to drop/stabilize.

Continued to tap up manually to 430A, 4.22V

Started out slow with a rate of ~10A/5min, and slowly increased to a rate of ~10A/min as vacuum stabilized, slowing down again when reaching carbonization outgassing.

Auto ramp at 0.2A/min from 430A-520A.


Thursday, March 29, 2018, 10:04

Reached 520A around 2am.

TGHT = 520A, 5.13V

IGP1 = 1.74e-6 Torr

Initiated auto-cool this morning at a rate of 1.0A/min.


 

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