Monday, May 11, 2015, 11:45
UO2/C green was prepared May 6, 2015. The slurry was cast on a piece of glass coated with WD40 on May 7, 2015.
The cast peeled off the glass nicely May 8, 2014 and finished drying over the weekend. [see attached picture]
Some materials were stuck on the WC jar wall and balls, consistent with every time.
Initial UO2 powder used = 50.44g (Inventory R-00835A, UO2 + bottle = 444.23g before use)
Graphite powder used = 10.05g
Green cast dried UO2/C + organic mass = 61.23g
The green was rolled up and wrapped in a piece of graphite sheet.
The Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.
Chamber is currently being pumped down.
Target boat will be ramped up to 520A at the rate of 0.1A/min
Vacuum limit stop at 5.0e-5 Torr, backing off at 6.0e-5 Torr.
Tuesday, May 12, 2015, 08:40
IG1 = 3e-6 Torr
Tapping up manually to 35A...
Tuesday, May 12, 2015, 12:18
Waited ~2.5hrs.
Vacuum stable.
IG1 = 1.3e-5 Torr.
Initiating auto-ramp.
Monday, May 25, 2015, 09:29
TGHT reached max setpoints on the 22nd.
IGP1 = 2.2e-6 Torr.
TGHT = 520A, 5.28V
Carbonization process is complete [see attachment].
Initiating auto-cool at 2.0A/min.
Wednesday, May 27, 2015, 08:47
Vented in argon and opened up yesterday afternoon.
Uranium flakes in glove box.
Wednesday, May 27, 2015, 16:09
UC2 flakes produced = 47.647g
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