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Message ID: 111     Entry time: Monday, May 11, 2015, 11:49
Author: Laura Lambert 
Target Material: UO2/C 
Target Oven W.O#: 40282-1 
Source: TARGET BOAT 
Status: Done 
Subject: Processing UC2Flk_06 

 Monday, May 11, 2015, 11:45

UO2/C green was prepared May 6, 2015. The slurry was cast on a piece of glass coated with WD40 on May 7, 2015.

The cast peeled off the glass nicely May 8, 2014 and finished drying over the weekend. [see attached picture]

Some materials were stuck on the WC jar wall and balls, consistent with every time.

Initial UO2 powder used = 50.44g (Inventory R-00835A, UO2 + bottle = 444.23g before use)

Graphite powder used = 10.05g

Green cast dried UO2/C + organic mass = 61.23g

The green was rolled up and wrapped in a piece of graphite sheet.

The Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber is currently being pumped down.

Target boat will be ramped up to 520A at the rate of 0.1A/min

Vacuum limit stop at 5.0e-5 Torr, backing off at 6.0e-5 Torr.


 Tuesday, May 12, 2015, 08:40

IG1 = 3e-6 Torr

Tapping up manually to 35A...


Tuesday, May 12, 2015, 12:18

Waited ~2.5hrs.

Vacuum stable.

IG1 = 1.3e-5 Torr.

Initiating auto-ramp.


 Monday, May 25, 2015, 09:29

TGHT reached max setpoints on the 22nd.

IGP1 = 2.2e-6 Torr.

TGHT = 520A, 5.28V

Carbonization process is complete [see attachment].

Initiating auto-cool at 2.0A/min.


 Wednesday, May 27, 2015, 08:47

Vented in argon and opened up yesterday afternoon.

Uranium flakes in glove box.


 Wednesday, May 27, 2015, 16:09

UC2 flakes produced = 47.647g


 

Attachment 1: IMG_20150508_143957199_HDR.jpg  3.284 MB  | Show | Hide all
Attachment 2: striptool.JPG  120 kB  Uploaded Monday, May 25, 2015, 10:34  | Hide | Hide all
striptool.JPG
Attachment 3: striptool-zoom.JPG  112 kB  Uploaded Monday, May 25, 2015, 10:34  | Show | Hide all
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