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Entry  Tuesday, September 23, 2014, 15:00, Laura Lambert, UO2/C, 40282-1, TARGET BOAT, In progress, Processing UC2Flk_04 
    Reply  Friday, October 10, 2014, 14:00, John Wong, UO2/C, 40282-1, TARGET BOAT, Done, Processing UC2Flk_04 archiver_TGHT&VAC.PNG
Message ID: 101     Entry time: Friday, October 10, 2014, 14:00     In reply to: 100
Author: John Wong 
Target Material: UO2/C 
Target Oven W.O#: 40282-1 
Source: TARGET BOAT 
Status: Done 
Subject: Processing UC2Flk_04 

Laura Lambert wrote:

 Tuesday, September 23, 2014, 14:54

UO2/C green was prepared Sept 18, 2014. The slurry was cast on a piece of glass coated with WD40 on Sept 19, 2014.

The cast was let dry over the weekend and peeled off the glass nicely Sept 22, 2014.

Some materials were stuck on the WC jar wall and balls as always noted.

Initial UO2 powder used = 50.04g (Inventory R-00835A UO2 + bottle = 544.51g before use)

Graphite powder used = 9.98g

Green cast dried UO2/C + organic mass = 59.35g

The green was rolled up and wrapped in a piece of graphite sheet.

The Ta-target boat is wrapped with 3-layers of heat shield and installed in Evap1.

Chamber is currently being pumped down.

Target will be ramped up to 520A at the rate of 0.1A/min

Vacuum limit stop at 5.0e-5 Torr, backing off at 6.0e-5 Torr.


 Wednesday, September 24, 2014, 11:27

Chamber pumped down overnight.

IGP1 = 2.3e-6 Torr

Manually stepping TGHT up to 30A


 Wednesday, September 24, 2014, 14:00

Vacuum stable.

IGP1 = 1.3e-5 Torr.

Initiating auto-ramp.


 

 Friday, October 10, 2014, 13:51

TGHT has reached to 520A for over 20hrs;  Carbonization process is complete (see attachment).

Ramping down at 2A/min. 

As much as I like to come to work, Monday is a holiday.  So, the chamber will be kept under vacuum. 

On Tuesday, the chamber will be vent in Ar. 


Friday, October 17, 2014, 11:47  

Vented and taken out on tuesday.


 

Attachment 1: archiver_TGHT&VAC.PNG  23 kB  | Show | Hide all
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